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Wednesday, September 30, 2020

My Educational philosophy

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My own philosophy of education intertwines with my own education, my life philosophy, and my upbringing. As one contemplates what the ultimate aim of education is and what that means to one's philosophy of education, this contemplation causes one to search for a deeper purpose and meaning to teaching and education. This contemplation has thus far brought me to a philosophy that is definitely an eclectic one.


This eclectic style and philosophy begins and ends with helping students develop the ability to think, contemplate, analyze, and question as independent, free thinking individuals. If one can accomplish this goal, one has helped develop an individual with the ability to develop new ideas and thoughts; as well as, question and evaluate both these ideas and thoughts and the ideas and thoughts of others. This type of education will produce an individual who listens, questions, agrees or disagrees but always is learning in some way. This philosophy is one that can coincide with most traditional educational philosophies whether behaviorism, essentialism, reconstructivism, or progressivism to list several; as it always charges the student to listen, question, contemplate, discover, and then agree or disagree with whatever philosophy, idea, problem, or solution that is presented or discusses. It also allows for all types of learning and learners as well as learning styles, since one only must listen, contemplate, discuss, discover, question, and then agree of disagree. In this philosophy, the teacher is a facilitator and guide. The teacher is not confined to teaching essentials, and imparting knowledge. He or she aids his or her students in analyzing, evaluating, constructing arguments, examining one's own and others ideas and beliefs, reflecting, and justifying ideas, beliefs, and solutions. This philosophy allows for change and disagreement. This allows one to act as a guide, in such a manner, allowing one's students to not only desire to learn past truths, solutions, knowledge, and ideas yet continually question, examine, analyze, reflect upon these truths, solutions, knowledge, and ideas. This reflection is indispensable in our society to discover new things, arrive at new solutions, in the end perpetuate, and improve upon the world and society in which we live.


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Tuesday, September 29, 2020

Christopher Columbus

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When Christopher Columbus landed in the Bahamas in 14, this started a series of great comparisons and contrasts between this explorer and others.


Columbus saw himself as a divinely religious person sent by God not to discover a new world, but to "be the messenger of a new heaven and a new earth" and that God would show him where to find it. His numerous religious observances and constant reminders to others that he was a "Christ-bearer" could make one conclude that this mystic is more of a medieval man, than a renaissance man. However, although Columbus might have been highly medieval in his ways, he was also a renaissance man as well. He studied heavily in the sciences of navigation, cosmology, and ancient texts, and like most renaissance men, dreamed of wealth and power.


Upon exploring the different islands, it seems that most every island Columbus claims, he claims for or names in honor of God or of the crown. This helps to justify Columbus' religious and honorable reasons for his explorations of what he thought was the Far East (India and China). It can be believed his letter and descriptions helped to justify his findings as well.


The way the "Indians" dressed (mostly naked) and their language difference may have also helped Columbus determine he was in East Asia. He also viewed the spices, gold, cotton, etc. (mainly gold) he received as his and his men's reward from God for his travels. Plus, the "Indians" viewed Columbus and his men as persons from heaven.


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Unfortunately, Columbus' findings were not completely accurate. The world was much larger than Columbus had anticipated, and it was not in the shape of a pear. He used his comparisons to medieval maps (based upon the Bible and other European explorer's reports), to constitute his findings about his bearings in the world. For an easier comparison, a child may think that a quarter past the hour is twenty-five minutes past the hour, since a quarter means twenty-five cents of a dollar. So if twenty-five cents is a quarter, why not twenty-five minutes? In both of these cases, the child and Columbus were right within their own reasoning, but generally wrong in the long run.


Columbus failed to fully realize this mistake throughout his life until his death, so sadly, if he had only corrected his way of thinking, the naming of the new nation (America), may have been reserved for him and this country may have been called Columbia, or Christophia, or some other fancy name.


I wonder too what Columbus could have done to prevent this mistake. Had he not traveled to Asia before? Would he not have thoroughly examined the explorations of others to Asia through the current trade routes and observe their descriptions of the Asian and Indian peoples and cultures? Would he not have had samples of writings and languages from there as well? Perhaps this would have prevented also the humiliation that was to be written into history.


Unlike his exploration predecessor, Amerigo Vespucci seems entirely a renaissance man. This nobleman born man was described as subtle, ironic, balanced and a rational sprit. He did not write about or claim to explore the new world for anyone or any specific reason, other than for pure scientific study.


If Vespucci mentioned attaining gold as a goal, it was quite rare. One would think that his less outspokenness of exploring for God, gold, and glory may have kept his head clear and might be a reason as to why his descriptions of the new world were more accurate. Columbus was probably so clouded with the thoughts of "I'm doing this for God, gold and glory," and was so outspoken about it, that he might have as well just said, "I'm doing this for me, me, me and it's mine, mine, mine." Vespucci did not do this, hence this left him better able to collect and analyze and observe the data in which he collected. So in the sense that "good things come to those to wait," Amerigo Vespucci's lack of aggressiveness to be in the spotlight of exploration, earned him the honor of a new nation being named for him.


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Monday, September 28, 2020

Patterns in Medicinal Advertising

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One of the most innovative trends in print advertising is medicine advertisement. The content of these particular advertisements (ads) are intriguing to me. I intend to analyze five medicinal ads to find the tools used by advertisers and to explore the positive and negative aspects of advertising medicine through print ads for the public.


The people who develop ads to market prescription medicine products must have an inkling of what the reader wants to see. For instance, the ads in a parenting magazine most often target mothers. The ads in a sports magazine predominately target athletes. How do the advertisers know what the reader will respond to?


Patterns are tools that help us to narrow our thinking down and put thoughts into categories that we identify with. Patterns allow us to store information in blocks so that we do not have to relearn information that has already been learned. Some patterns are universal and most people have some categories or patterns that other people have. An example of a universal human pattern is using language to communicate. Other patterns that we have, may be derived from our own experience and unlike those of others. Patterns are useful in advertising because advertisers can target their reader by tapping into specific categories.


Perception is a persons understanding of the information they receive. Depending on their experience or their understanding they will categorize their perception and in turn it will become a thought pattern. For instance when a person talks to a priest their perception of him may be that he is perfect or does not sin. They may categorize all priests this way and not judge them in the way that they would any person who is not a priest. I feel that patterns and perception work hand in hand. Sometimes patterns are formed based on perception, sometimes perception is based on a pattern. What came first the chicken or the egg? Im not quite sure, but I do know they affect each other. Ads are designed by using patterns that target a specific audience. The readers perception of the product may form exclusively based on the ad.


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The patterns that I noticed specifically amongst the five medicine ads that Ive chosen to analyze is the break through effect. In one ad there was a woman with her child and they were breaking through glass. Another ad featured a woman and her child with clear blue skies breaking through the clouds above. The third ad has a man skiing through a mountain of wild flowers.


The thought of breaking through something with a smile is somewhat encouraging and enticing. Thus a reader might perceive this medicine as exciting so they may ask their doctor for this kind rather than another kind that has been useful to them in the past. The thought of carelessly skiing over wildflowers is also exciting and visually euphoric.


The coloring used in the ads is captivating. One ad has a sunset with the colors creating a relaxed feeling. Brown is seems to set a pattern as an offset color in four of the five ads. Sky blue is also used, it looks uplifting and freeing.


Another pattern that I noticed is the use of perfect children in the ads. These children do not have a hair out of place or a speck of dirt on their clothing. Both the mothers and the children in the ads are smiling and seemingly relaxed. In other words a persons perception of the product could be that taking this medicine would create clean, relaxing family harmony. The ads also suggest calling a toll free number to receive a coupon or rebate


check upon purchase of their product. This is a wonderful way to get the readers attention, as most people respond to price reductions whether they know the product or not.


There is also a pattern of listing how many times a day the medicine needs to be administered. These ads make reference to the difference in dosage between other medicines as compared to theirs. They focus on the convenience of taking the medicine.


All five of my ads list the possible side effects and teratogens as well as harmful drug interactions on the backside of the ad in fine print. This information definitely does not grab the readers attention as the picture on the front does. The advertisers most likely assume that the picture alone will sell their product. Some of the ads do list possible side effects on the front of the ad in small print as well.


It is clear to me that the advertisers have a perception of how the patterns will influence the reader. The readers perception of the medicine is based purely on what the eye can see. They cant feel, taste, smell or sample the medicine from looking at an advertisement. Therefore their perception of the ad has absolutely nothing to do with the actual product and its effectiveness or ineffectiveness.


Prescription medicine is not something that should be chosen spontaneously or without researching the product. Often times the medicine can be prescribed by a doctor based solely on the patients request. The patient most likely does not know enough about the medicine if they are requesting it based on the advertisement.


It is unfortunate that advertisers go to such lengths to sell products. It is equally unfortunate that people respond to the advertisements based on a picture or a feeling that they get because of the presentation. The reason that I feel that its unfortunate is because prescription drugs can be very harmful if not taken seriously and with caution. If a product cannot be sold in a store, by mail, or in a catalog without a doctors prescription does it


belong as an advertisement in a magazine? I assume this is a somewhat controversial issue between pharmaceutical companies and doctors who are uncomfortable with overexposing medicines by using catch phrases or visual stimulus. It undermines the importance of a doctors role in diagnosing and treating individuals.


The positive aspects of advertising medicine in magazines are beneficial to the pharmaceutical companies especially. They create allure to their product by using patterns to interest the reader and therefore the reader is more likely to request their medicine as a result. This benefits the sales and notoriety of the product. The one positive way that this form of advertising can benefit the reader is if they have an existing problem and they dont know theres a treatment for it. It could open a door for the reader to contact their doctor about it.


It is apparent to me that the advertisers use many patterns based on their perception and what they assume will be the perception of the reader. The advertisers must have enough information on what specific patterns the reader will respond to because they do a good job of capturing the readers attention. Despite my opposition of advertising medicine this way, it is interesting to have discovered the tools used in doing so.


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Friday, September 25, 2020

BANK z (A HYPOTHETICAL CASE)

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CASE STUDY SERVICE INDUSTRY (Bank Z)


General Background


Bank Z is the largest domestic private sector bank in India. Since its inception in 10 till date, the bank takes a pride in serving its three million customers through a vast domestic network of seventeen regions consisting of 6 branches and 101 extension counters spread across the length and breadth of country. The total manpower strength of the bank stands at 5877, out of which 780 are workmen. Financially, the bank has been doing moderately well with increasing trend of deposits and profits level. In the face of deregulation (Narasimham Committee Recommendations), stiff competition and volatility in markets, the bank had to opt for reorienting its strategic framework by introducing strategic intents like sustained profitable growth, training/upgradation of human skills, enhanced customers', shareholders' and employees' satisfaction, leverage IT and branch network, focus on retail banking, establishment of strong customer relationships etc to retain the leading position among the private sector banks. These strategies were to be driven by measures such as diversification, joint ventures, customer service, cost reduction, restructuring etc.


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Assessment of Environment


The external environment of Bank Z is undergoing a rapid transformation. Among many of the external environment, the bank is facing the direct implications of following three key triggers


• Government Policy Changes The implementation of liberalized policy by the government has created favorable environment for the banking sector. Such as deregulation of interest rate structure has given flexibility to the banks to fix its own rate of interest. Reduction of government stake to percent has led to opportunity of having more power to the management team of the bank regarding the decision making etc.


• Intensification of Competition The impact of liberalized government reform is seen in the form of intensified competition in the banking sector. The entry of foreign banks and new private sector has increased the competition and complexity in the domestic banking sector. As a result, an extra effort needs to be made by every bank in order to achieve adequate level of growth and profitability in order to survive the rage of volatility due to stiff competition.


• Technological Change In order to move ahead in the competition, one of the strategic responses of Bank Z is leverage information technology and branch network. Introduction of more customized products such as Automatic Teller Machines (ATMs), Tele Banking Counters (TBCs) and Automating Forex services requires development of sophisticated technological packages. Thus, Bank Z needs to prepare well ahead to make necessary move to muddle through the IT jungle to meet the needs of the changing situation.


Corporate Strategies Identification


Corporate Strategy means an overall managerial move/game plan for the whole organization. With the deregulation, the bank has realized the need to reorient its corporate strategy. It has started articulating a theme for every fiscal year to excel in its operations and gain maximum business advantage. As for instance we can see the bank working on the theme of "sustained profitable growth" or "diversified and balanced business portfolio" during two different fiscal years. The bank has responded by evolving three different forms of Strategic Responses lately to retain the leading position among the private sector banks. These three Strategic modes are;


N Strategic responses related to portfolio management


N Strategic responses related to Process management


N Strategic responses related to Structure in the Bank.


Strategic responses related to portfolio management


Diversification By 00 the bank proposes to diversify into the following areas of business


N Consumer Finance


N Mutual Funds


N General Insurance


Joint Venture In order to expand its operations the bank is trying to form joint ventures with some international players.


Collaboration In order to launch insurance operations in India, the bank is negotiating with major European Insurance Company.


Strategic responses related to Process management


Its process related strategies consists of giving increased services to its customers such as introduction of ATM, extension of business hours at Tele Banking Counters (TBCs), Rejuvenation of customer service committee etc. Similarly it also includes marketing strategies like brand building, advertisements, up gradation of skills etc.


It also aims at providing various information technologies like email facility to 00 locations, CMS to 50 locations, Automating Forex Services etc. It also has a cost reduction strategy and the bank also has a quality strategy, which includes good inspection system, adherence to customer service manual and customer satisfaction.


Strategic responses related to Structure in the Bank


The Bank has introduced flat structure in place of its hierarchal structure and also has introduced a profit centre concept, which means that each region is a profit centre and is accountable for its business performances.


Identification and Assessment of HRD Responses


The Bank has a wide array of HRD process and responses provided to its employees which are identified as hereunder;


N Compensation is according to IBA's guidelines and also consistent with Consumer Price Index rate. A wide range of allowance and perks has been arranged. They are also entitled to receive soft loans, such as house building advance, vehicle loan, various policies and holiday advance. They also get statutory benefits like bonus, social security schemes etc.


N Working Conditions is excellent with no compromise made on any aspect. The bank emphasize on the congenial physical environment in the bank to attract the customers and to provide a comfortable working place.


N Family welfare Employees are well taken care of with the Family Welfare provision The bank provides medical aid to the dependent family member. The employees are also paid education allowance and each employee along with the dependent family members is entitled for leave travel concession and has also introduced a pension scheme.


N No proper written HR Policy inspite of having full-fledged HR Department However it has a few booklets containing rules and regulations governing the sanction of advances and service rules.


N Training policy yet not evolved. But it follows a custom of training every employee a minimum of two or three days in a year and has a full-fledged training infrastructure at Bangalore.


N No written Performance Appraisal System Even though the bank has a performance appraisal format it has no written appraisal policy.


N Job Enrichment The Bank does not have a specific programmes/effort designed or implemented to enhance the job content of the staff except a kind of job rotation system which is yet not clear.


N Career Planning The Bank does not have any formal career planning.


N Communication In order to make the employees aware of various important developments, new policies and business plans, the bank publishes a monthly newsletter. No other communication mechanism is used in Bank Z.


N Employee involvement and empowerment programmes The bank has started a quality circle, which has been adopted by many branches. Except QC, no other employee participation programs are there in the organization.


Alignment


Analyzing the present policies and practices adopted at the bank and then comparing it to the Corporate Strategy, we can deduce that though the bank seems to be providing wide array of employee perks, allowance and benefits, it does lack in few aspects in alignment of its HR practices to that of Corporate Vision and Strategy.


N According to the Corporate Vision, Employee Growth is taken as a Commitment; however the conspicuous absence of any definite specific HR Policy inspite of having full-fledged HR Department shows the commitment is not very serious. Similarly, the managements apathy for upgrading the skills of clerical staff beyond a certain level in consideration of the fear that the highly skilled workers may leave the bank after they are upgraded is nothing but because of the lack of proper HR and Training Policy. The bank should instead ensure that its employees are skilled and are the best in the industry to provide the seamless service to its customers and better than its competitors are providing.


N One should not forget that the quality service is a core competency of the banks which is only possible when the employees, who come to direct contacts with the clients and customers, give high level of performance. The quality of performance can be ensured by the regular performance appraisal. Performance Appraisal in service sector like Bank Z is something which one cannot afford to ignore because it helps to improve the individual, team and groups performance by identifying the areas needed for improvement and help the organization as a whole to gain its objectives by improved service and performance. But at Bank Z it seems that Performance Appraisal is done just for the sake of doing it. No formal policy, authority or trained officer takes charge of the process. Though the PA system is used for the purposes of training, promotions, and placement in a particular function, due to lack of trained authority, counseling and further improvements required are not taken into consideration seriously.


N There is no formal career planning carried out in the bank. Though there is a scheme to encourage staff to acquire additional qualification and provision that employees acquiring these qualifications will be rewarded with monetary incentive and earn extra credit points for promotion to higher posts, which is just for short run. But no formal development needs of employee for long run are identified.


N The HRD practices where Bank Z is good at; such as Compensation, Working Conditions and Family Welfare can only fulfill the basic physiological needs of an employee. Moreover, it seems that bank had these facilities only because of unions influence to the management. The challenges at work and self actualization needs of the employees cannot be fulfilled by these mere compensation packages. For this, job enrichment and employee participation in decision making is required which the bank seems to be lacking. For job enrichment, they have only job rotation program which still is not coherent. Giving a common designation irrespective of actual job profile with less hierarchical level may give less development ladder to the employees which may act adversely as demotivating factor for ambitious employees. Similarly, the bank has QC program as employee participation and empowerment program which do help the employee to solve work related problems; yet employees are not participated in decision making of the organization.


N Similarly, the bank lacks two way communications between management and employee. Employees are informed only through the newsletter published monthly. There is no way the employee can give their opinion to the management.


Suggestions/ Conclusion


 The bank needs to have a separate HRD Vision and Strategies consistent with the corporate strategy, vision and mission.


 The bank should craft effort to make business strategy and employee resource strategy coherent to each other.


 A push for a more business-driven thrust to HRD at organisational level is needed because HRD Strategy is something, which falls, at functional strategy level. Though it is narrower in scope compared to overall business strategy, it adds relevant details to the overall business game plan. Care should be taken that the HRM Strategy must support the bank's overall business strategy and competitive approach.


 The bank should Improve HRD not only Employee Development because there are individuals or groups who have some relationship with an organisation but are not in an employer-employee relationship. These external people and institutions have a direct or indirect interest in the business and influence the success of the business.


 The bank come up with formal exhaustive HR Policy including training policy ensuring that the employees are well trained and those on whose training investment is done cannot leave the bank all of a sudden to join competitors bank.


 The Bank is to face a stiff competition from influx of foreign banks and their powerful resources and thus to ensure the retention of its highly qualified executives from joining those foreign banks the bank could provide Employee Stock Options to the deserving workforce of the bank.


 Efforts to increase the client base and to retain the customers should be instilled while formulating the plans and procedures by providing better facilities and products than the competitors. One of the ways of outperforming competitors is to increase performance of employees to give better customer service; for which HR capital should be mobilized efficiently giving them more than compensation in terms of job enrichment, communication and participation at policy level.


 Similarly, attempt should be made to roll out the latest in technology like internet-banking and train the staffs and customers to use it efficiently.


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Thursday, September 24, 2020

Huswifery

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Crystal dela Plata


English 01


Mrs. Kohli


An Analysis of Edward Taylor's poem "Huswifery"


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"Huswifery" is a poem written by Edward Taylor. Edward Taylor was most likely born in 164, in Leicestershire, England (Rowe 456). He was the son of a yeoman farmer and studied at Cambridge University (Rowe 456). "As a preacher and a Puritan, […], Talyor felt spiritually unworthy of God's grace" (Rowe 458). This is seen through his peotic works as he uses different metaphysical conceits in each of his poems to show his love for God, as well as, the collective aspects of his spirituality. Edward Taylor uses metaphysical conceit in his poem "Huswifery" to portray each of his spiritual blessings as a part of the whole of himself through the art of weaving.


Taylor uses the art of weaving as metaphysical conceit to describe each spiritual part of his self as a tool being spun for God's use. Taylor already feels unworthy of God's grace; he is simply asking to be used of God. In the poem Taylor writes, "Make mee, O Lord, thy Spining Wheele compleat" (1). Here Taylor is using metaphysical conceit to allude that his soul is the Spining Wheele and he is pleading for God to make his soul complete within Christ. He is recognizing that he needs God to make him complete. Taylor then asks God to make "Thy Holy Words my Distaff make for mee / Make mine Affections thy Swift Flyers neate" (-). Taylor is comparing God's holy words to the distaff of a spinning wheel, which "holds the flax or raw wool" (Lauter 467). He wants God's words to be the stability that holds him up and keeps him going for God's glory. His is also saying let my affections be those of your affections. He also use metaphysical conceit to compare his soul to the spool and his conversation to the reel when he says, "And make my Soule they holy Spoole to bee. / My Conversation to be thy Reele" (4-5). His soul is the spool on which he wants God's blessings to be spun and for them to be spun his conversation has to be the reel on which God's message is sent. Taylor also writes, "Then weave the Web thyselfe. The yarn is fine. / Thine Ordinances make my Fulling Mills" (-11). Here Taylor is referring to God's ordinances or laws as the tools to make him full, or also humble and strong in God's word so Satan or temptation does not ever win in his life. Or simply, to make His laws known to Taylor so that Taylor does not ever sin against him. In the end of the poem he sums it all up literally as


…cloath therewith mine Understanding, Will,


Affections, Judgment, Conscience, Memory


My Words, & Actions, that their shine may fill


My wayes with glory and thee glorify.


Then mine apparel shall display before yee


That I am Cloathd in Holy robes for glory (1-18).


Here Taylor is summing up what is said in the first two stanzas. He is insinuating that all of these, his understanding, will, affections, judgment, conscience, memory, words and action will come together as one with God's guidance to glorify God in everything he does. He is also making a typological reference to the garments of salvation and robes of righteousness talked about in Isaiah 1610. He wants his whole body to be model of Christian charity.


In conclusion, Edward Taylor uses metaphysical conceit in his poem "Huswifery" to compare each aspect of his character to a part of the tools used for weaving. Taylor does this to make a reference to his self as a tool being used for God's glorification. He want to give God the glory not only externally through his words and actions, but also internally through his understanding, judgment, and conscience, just to name a few, so that his can grow in God's grace to become and stay one of God's chosen elect. He uses metaphysical conceit to weave a poem that will garment God's greatness, as well as, his desire to be used for God.


Works Cited


Lauter, Paul, Ed. The Heath Anthology of American Literature. 5th ed., vol. 1. New York W.W. Norton, 18.


Rowe, Karen E. "Edward Taylor 164?-17". Paul Lauter, Ed. The Heath Anthology of American Literature. 5th ed., vol. 1. New York W.W. Norton, 18. (456-45).


Taylor, Edward. "Huswifery". Paul Lauter, Ed. The Heath Anthology of American Literature. 5th ed., vol. 1. New York W.W. Norton, 18. (467-468).


Please note that this sample paper on Huswifery is for your review only. In order to eliminate any of the plagiarism issues, it is highly recommended that you do not use it for you own writing purposes. In case you experience difficulties with writing a well structured and accurately composed paper on Huswifery, we are here to assist you. Your persuasive essay on Huswifery will be written from scratch, so you do not have to worry about its originality.


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Wednesday, September 23, 2020

Controversial topics for essay

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Tuesday, September 22, 2020

Eulogy

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Abstract


Two unknowns were attempted to be identified by a series of solubility tests, followed by a series of functional group tests. Derivatives of the compounds were to be formed to confirm the identity of the substances. The solid did not have a melting point, rather, it sublimed. The solid and liquid were tested for solubility in water, 5% NaOH, 5% NaHCO, 5% HCL, and HSO4. The liquid was found to have a boiling point of 184°C. The liquid was tested using the beilstein test for halogens, the ferric chloride test for phenols, ,4-DNP for carbonyls, Br/CCl4 for multiple bonds, and the Tollens test for aldehydes. No derivative could be formed with the liquid because the sample evaporated. It was concluded that the liquid was benzaldehyde, which has a BP of 17°C.


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Introduction


Qualitative analysis of unknown compounds is based on functional group chemistry. Several different classification tests can be performed on a substance to determine the functional groups that are present, or absent for that matter. For example, the Beilstein test, tests for halogens. A copper wire is heated and then coated with the sample and then heated again. If a green flame is present, this is a positive result. The green flame is the result of the production of a volatile copper halide ().


The most important tests that should be performed initially are the solubility tests. These tests give important information about the functional groups present. For example, compounds that contain 4 or less carbons, and contain oxygen, nitrogen, or sulfur are usually soluble in water (). A flow chart on page 44 of the lab text outlines the procedure to follow for the solubility tests. Identity of unknown compound can be concluded by logical elimination of certain functional groups, and by using the results of each classification test to narrow the possibilities.


Results and Discussion


The tests and results for the solid unknown #6 are located in table 1.


Table 1


Solubility tests


According to the chart on p. 44 of the lab text, the solid probably does not have a low molecular weight, and is not a carboxylic acid or amine because it was not soluble in water. Furthermore, it was also indicated that it is not a carboxylic acid because it was not soluble in NaOH. NaOH insolubility also suggests it is not a phenol. The solid was not soluble in HCl, which suggests it is not a base, such as an amine. The solid was soluble in HSO4, which indicates that the solid is a neutral compound, or inert.


Possibilities based on solubility tests


· Alkenes


· Alcohols


· Ketones, aldehydes


· Nitro compound


· Esters, ethers


· Alkyl halides


· Aromatic compound


Classification tests


The solid was first tested for multiple bonds to eliminate or indicate an alkene. The tests is based on the reactivity of a double bond with the addition of bromine


The solution of Br/CCl4 and the solid did not become colorless, which indicates that the compound does not contain a multiple bond between carbons.


The solid was then tested for an aldehyde or ketone with the ,4-DNP test. The color of the precipitate formed is used as a guide to the type of functional group present. A yellow precipitate usually indicates an unconjugated ketone or aldehyde (). A red precipitate indicates conjugation. The solid tested produced a yellow-orange precipitate. From the results of the saturation test, which suggested no multiple bonds, it can be concluded that the solid may be an unconjugated aldehyde or ketone.


The Tollens test was used to differentiate between an aldehyde and a ketone because of the highly positive ,4-DNP test. The Tollens test is based on the fact that aldehydes normally produce a precipitate of silver metal by reduction of ammoniacal silver nitrate


The solid did produce a heavy silver precipitate on the sides of the glass test tube. Because ketones do not normally react in this test, one can conclude the solid is an aldehyde.


Derivative formation


It was concluded from the classification tests that the solid is an aldehyde, however no derivatives were formed. ,4-DNP and semicarbazone were attempted to be produced. The procedure for ,4-DNP was repeated twice with extra precision. Upon consultation with Mrs. Collins, the lab manager, it was concluded that the second batch of ,4-DNP was contaminated or produced incorrectly. The second batch was compared to the first and they were clearly different. There was not enough time to repeat the procedure a third time with new ,4-DNP.


The solid did appear to have a melting point. The melting point was attempted of the Fisher-Johns apparatus and the Mel-Temp apparatus twice. The solid appeared to sublime, which occurs when a solid goes directly to the vapor phase. This may have occurred because the vapor pressure of some solids depends on the temperature of the surroundings.


According to the appendix of derivatives on p. A of the lab text, the most likely possibility for the compound is pentanal. This was concluded because it was the only aldehyde that did not for semicarbazone. Also, according to the HO solubility test, the solid most likely has more than 4 carbons. Pentanal is not conjugated and has no double bonds, which was suggested by the ,4-DNP and the saturation test. The structure for pentanal is


Table


Test Positive result Result Comment


Solubility tests


The liquid was soluble in water, which suggests the compound contains 4 or less carbons, and may contain O, N, or S. If a compound is soluble in water, the Ph of the liquid should be considered. The liquid did not change the color of the red or blue litmus paper, so the compound is neutral. The compound was soluble in both NaOH and NaCO, which indicates a phenol, or carboxylic acid.


Possibilities based on solubility tests


· Carboxylic acid


· Phenol


· Low MW neutral compound


Classification tests


The liquid was tested for a phenol with the ferric chloride test. Red, Blue, or purple colors are produce in this test from the formation of complex phenols with the Fe(III) ion (). The liquid did not produce any colors. The liquid was then tested for the presence of a halogen with the Beilstein test. The Beilstein test is positive with the production of a green flame. The color is produced from the formation of a copper halide (). This test was also negative.


Because the litmus test indicates a neutral compound, and the ferric chloride test eliminated the possibility for a phenol, the liquid was tested for an aldehyde or ketone. The solubility of the unknown in water may have been due to the presence of a double bonded O. The ,4-DNP test was positive for the presence of a carbonyl. Furthermore, the Tollens test was positive for an aldehyde, giving the same result as the unknown solid. The saturation test, Br/CCl4, was positive for multiple bonds.


No derivatives could be made with the liquid because the sample appeared to have evaporated. Based on the BP of 184°C, and the above data, the unknown was concluded to be benzaldehyde, which has a BP of 17°C


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